8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

Base Information

Chemical Name:8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine
CAS No.:159150-89-7
Molecular Formula:C₂₈H₂₇N₃O₂
Molecular Weight:437.541
Hs Code.:

Synonyms:8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

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Chemical Property of 8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

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Technology Process of 8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

There total 4 articles about 8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1539-42-0
bis[(2-pyridyl)methyl]amine

: 159150-88-6
8-(bromomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

: 159150-89-7
8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

Guidance literature:: With sodium hydride; In dichloromethane; for 48h;
DOI:10.1016/0040-4039(94)88214-2

Reference yield:

: 91-04-3
2,6-bis(hydroxymethyl)-4-methylphenol

: 159150-89-7
8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 5.5 h / 50 °C

2: 75 percent / CBr₄, PPh₃ / dimethylformamide / Ambient temperature

3: 86 percent / NaH / CH₂Cl₂ / 48 h

With carbon tetrabromide; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)88214-2

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 159150-89-7
8-(bis(2-pyridylmethyl)aminomethyl)-6-methyl-2-phenyl-2,4-dihydro-1,3-benzodioxine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 5.5 h / 50 °C

2: 75 percent / CBr₄, PPh₃ / dimethylformamide / Ambient temperature

3: 86 percent / NaH / CH₂Cl₂ / 48 h

With carbon tetrabromide; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)88214-2