4-methyl-3-(2-methylamino)ethyloxynitrobenzene

Base Information

Chemical Name:4-methyl-3-(2-methylamino)ethyloxynitrobenzene
CAS No.:916737-61-6
Molecular Formula:C₁₀H₁₄N₂O₃
Molecular Weight:210.233
Hs Code.:

Synonyms:4-methyl-3-(2-methylamino)ethyloxynitrobenzene

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Chemical Property of 4-methyl-3-(2-methylamino)ethyloxynitrobenzene

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Technology Process of 4-methyl-3-(2-methylamino)ethyloxynitrobenzene

There total 3 articles about 4-methyl-3-(2-methylamino)ethyloxynitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 575474-36-1
N-methyl-2-(2-methyl-5-nitrophenoxy)acetamide

: 916737-61-6
4-methyl-3-(2-methylamino)ethyloxynitrobenzene

Guidance literature:: N-methyl-2-(2-methyl-5-nitrophenoxy)acetamide; With boron dimethyl-trifluoro sulphide; In tetrahydrofuran; at 0 - 20 ℃; for 2.08333h; Heating / reflux;

With hydrogenchloride; methanol; at 60 ℃; for 2.5h;

With ammonia; In methanol;

Reference yield:

: 5428-54-6
2-methyl-5-nitrophenol

: 916737-61-6
4-methyl-3-(2-methylamino)ethyloxynitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 24 h / 20 °C / Heating / reflux

2.1: N-ethyl-N,N-diisopropylamine / methanol / 6 h / 90 °C

3.1: boron dimethyl-trifluoro sulphide / tetrahydrofuran / 2.08 h / 0 - 20 °C / Heating / reflux

3.2: 2.5 h / 60 °C

With boron dimethyl-trifluoro sulphide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; acetone;

Reference yield:

: 90923-04-9
methyl 2-(2-methyl-5-nitrophenoxy)acetate

: 916737-61-6
4-methyl-3-(2-methylamino)ethyloxynitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / methanol / 6 h / 90 °C

2.1: boron dimethyl-trifluoro sulphide / tetrahydrofuran / 2.08 h / 0 - 20 °C / Heating / reflux

2.2: 2.5 h / 60 °C

With boron dimethyl-trifluoro sulphide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;