Technology Process of 4-methyl-3-(2-methylamino)ethyloxyaniline
There total 4 articles about 4-methyl-3-(2-methylamino)ethyloxyaniline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
methanol;
for 4h;
under 2068.65 Torr;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: boron dimethyl-trifluoro sulphide / tetrahydrofuran / 2.08 h / 0 - 20 °C / Heating / reflux
1.2: 2.5 h / 60 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 2068.65 Torr
With
boron dimethyl-trifluoro sulphide; hydrogen;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 24 h / 20 °C / Heating / reflux
2.1: N-ethyl-N,N-diisopropylamine / methanol / 6 h / 90 °C
3.1: boron dimethyl-trifluoro sulphide / tetrahydrofuran / 2.08 h / 0 - 20 °C / Heating / reflux
3.2: 2.5 h / 60 °C
4.1: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 2068.65 Torr
With
boron dimethyl-trifluoro sulphide; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; acetone;
