(S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid

Base Information

• Chemical Name: (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid
• CAS No.: 1373233-98-7
• Molecular Formula: C₂₆H₃₂N₂O₆
• Molecular Weight: 468.55

Synonyms:(S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid

Chemical Property of (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid

Chemical Property:

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Technology Process of (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid

There total 1 articles about (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H22N2O4 → (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid (1373233-98-7)

Guidance literature:

C₁₁H₂₂N₂O₄; N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide; With N-ethyl-N,N-diisopropylamine; In water; acetonitrile; at 20 ℃;

With hydrogenchloride; In water; acetonitrile;

DOI:10.1016/j.bmc.2012.02.033

Reference yield:

2-chlorotrityl resin + (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid (1373233-98-7) + Fmoc-Ser(tBu)-OH (71989-33-8) → C68H103ClN9O15Pol

Guidance literature:

2-chlorotrityl resin; Fmoc-Ser(tBu)-OH; With benzotriazol-1-ol; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; solid phase reaction;

(S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid; Further stages;

DOI:10.1016/j.bmc.2012.02.033

Reference yield:

2-chlorotrityl resin + N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + (S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid (1373233-98-7) → C58H83ClN9O13Pol

Guidance literature:

2-chlorotrityl resin; N-(fluoren-9-ylmethoxycarbonyl)glycine; With benzotriazol-1-ol; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; solid phase reaction;

(S)-5-[N-acetyl-N-(tert-butoxy)amino]-2-[N-(9-fluorenylmethoxycarbonyl)amino]pentanoic acid; Further stages;

DOI:10.1016/j.bmc.2012.02.033

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