Technology Process of C29H36F6N2O3
There total 9 articles about C29H36F6N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride; acetic acid;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / Heating
2: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride
3: hydrogen / palladium on activated charcoal / methanol
4: 3-chloro-benzenecarboperoxoic acid / dichloromethane
5: diisobutylaluminium hydride
6: Dess-Martin periodane / dichloromethane
7: sodium cyanoborohydride; acetic acid / dichloromethane / 20 °C
With
hydrogen; diisobutylaluminium hydride; sodium cyanoborohydride; sodium carbonate; Dess-Martin periodane; acetic acid; 3-chloro-benzenecarboperoxoic acid;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal;
In
methanol; 1,2-dimethoxyethane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: potassium carbonate; iodine / water
2: caesium carbonate
3: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / Heating
4: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride
5: hydrogen / palladium on activated charcoal / methanol
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane
7: diisobutylaluminium hydride
8: Dess-Martin periodane / dichloromethane
9: sodium cyanoborohydride; acetic acid / dichloromethane / 20 °C
With
hydrogen; iodine; diisobutylaluminium hydride; sodium cyanoborohydride; sodium carbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; acetic acid; 3-chloro-benzenecarboperoxoic acid;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal;
In
methanol; 1,2-dimethoxyethane; dichloromethane; water;