N-(cyclohex-2-en-1-yl)benzenesulfonamide

Base Information

• Chemical Name: N-(cyclohex-2-en-1-yl)benzenesulfonamide
• CAS No.: 108223-53-6
• Molecular Formula: C12H15 N O2 S
• Molecular Weight: 237.323
• Hs Code.: 2935009090
• DSSTox Substance ID: DTXSID40544973
• Nikkaji Number: J1.806.336K
• Mol file: 108223-53-6.mol

Synonyms:108223-53-6;N-cyclohex-2-en-1-ylbenzenesulfonamide;Benzenesulfonamide, N-2-cyclohexen-1-yl- (9CI);N-(cyclohex-2-en-1-yl)benzenesulfonamide;N-(2-Cyclohexen-1-yl)benzenesulfonamide;DTXSID40544973

Chemical Property of N-(cyclohex-2-en-1-yl)benzenesulfonamide

Chemical Property:

• PSA: 54.55000
• LogP: 3.54530
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 237.08234989
• Heavy Atom Count: 16
• Complexity: 337

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC=CC(C1)NS(=O)(=O)C2=CC=CC=C2

Technology Process of N-(cyclohex-2-en-1-yl)benzenesulfonamide

There total 8 articles about N-(cyclohex-2-en-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

benzenesulfonamide (98-10-2) + cyclohexa-1,3-diene (1165952-91-9) → N-(cyclohex-2-en-1-yl)benzenesulfonamide (108223-53-6)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; tetrakis(actonitrile)copper(I) hexafluorophosphate; 1,2-bis-(diphenylphosphino)ethane; In 1,4-dioxane; at 50 ℃; for 3h;

DOI:10.1021/ja056112d

Reference yield: 75.0%

benzenesulfonamide (98-10-2) + cyclohexene (110-83-8) → N-(cyclohex-2-en-1-yl)benzenesulfonamide (108223-53-6)

Guidance literature:

With tert.butyl-peroxyacetate; 4 A molecular sieve; copper(II) bis(trifluoromethanesulfonate); 1,10-Phenanthroline; In 1,2-dichloro-ethane; at 60 ℃; for 6h;

DOI:10.1021/ol062514u

Reference yield: 50.0%

bis(N-sodiophenylsulfonylamino)selenium dichloride (108223-43-4) + cyclohexene (110-83-8) → N-(cyclohex-2-en-1-yl)benzenesulfonamide (108223-53-6)

Guidance literature:

In 1,2-dichloro-ethane; at 20 ℃; for 48h;

upstream raw materials:

bis(N-sodiophenylsulfonylamino)selenium dichloride

cyclohexene

N-benzenesulfonyl-7-azabicyclo<4.1.0>heptane

benzenesulfonamide