1-BUTYL-2,3-DIMETHYLIMIDAZOLIUM IODIDE

Base Information

• Chemical Name: 1-BUTYL-2,3-DIMETHYLIMIDAZOLIUM IODIDE
• CAS No.: 108203-70-9
• Molecular Formula: C9H17 N2 . I
• Molecular Weight: 280.152
• Hs Code.: 2933290090
• Mol file: 108203-70-9.mol

Synonyms:1H-Imidazolium,1-butyl-2,3-dimethyl-, iodide (9CI); 1-Butyl-2,3-dimethylimidazolium iodide

Chemical Property of 1-BUTYL-2,3-DIMETHYLIMIDAZOLIUM IODIDE

Chemical Property:

• PSA: 8.81000
• LogP: -1.57490

Purity/Quality:

98%min ^*data from raw suppliers

1-BUTYL-2,3-DIMETHYLIMIDAZOLIUM IODIDE 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-BUTYL-2,3-DIMETHYLIMIDAZOLIUM IODIDE

There total 3 articles about 1-BUTYL-2,3-DIMETHYLIMIDAZOLIUM IODIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,2-dimethyl-1H-imidazole (1739-84-0) + 1-iodo-butane (542-69-8) → 1-n-butyl-2,3-dimethylimidazolium iodide (108203-70-9)

Guidance literature:

In 1,1,1-trichloroethane; at 40 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c5ra09688j

Reference yield: 78.0%

→ 1-n-butyl-2,3-dimethylimidazolium iodide (108203-70-9)

Guidance literature:

In acetonitrile; at 80 ℃; for 12h;

Reference yield:

1-butyl-2,3-dimethylimidazolium bromide → 1-n-butyl-2,3-dimethylimidazolium iodide (108203-70-9)

Guidance literature:

With Amberlyst A-26 (I^- form); In methanol;

DOI:10.3390/molecules17044007

upstream raw materials:

1,2-dimethyl-1H-imidazole

1-iodo-butane

Downstream raw materials:

1-butyl-2,3-dimethylimidazolium bis-(trifluoromethanesulfonyl)amide

1,2-dimethyl-3-butylimidazolium bromodiiodide

1-butyl-2,3-dimethylimidazolium dibromoiodide

Refernces

• 1、 Kutuniva, Johanna,Oilunkaniemi, Raija,Laitinen, Risto S.,Asikkala, Janne,K?rkk?inen, Johanna,Lajunen, Marja K.. "Synthesis and structural characterization of 1-butyl-2,3-dimethylimid- azolium bromide and iodide". . p. 868 - 870. Retrieved 2007.
• 2、 -. "Alkali stability excellent imidazole and imidazolium cation". Paragraph 0243-0244; 0305-0307. . Retrieved 2018/04/13.