IODOBIS(INDENYL)VANADIUM(III)

Base Information

• Chemical Name: IODOBIS(INDENYL)VANADIUM(III)
• CAS No.: 108150-19-2
• Molecular Formula: C₁₈H₁₄IV
• Molecular Weight: 408.155
• Hs Code.: 2931900090
• Mol file: 108150-19-2.mol

Synonyms:IODOBIS(INDENYL)VANADIUM(III)

Chemical Property of IODOBIS(INDENYL)VANADIUM(III)

Chemical Property:

• Melting Point: >300 °C(lit.)
• PSA: 0.00000
• LogP: 5.68430

Purity/Quality:

99% ^*data from raw suppliers

Iodobis(indenyl)vanadium(III) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 23/24/25-36/37/38
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of IODOBIS(INDENYL)VANADIUM(III)

There total 1 articles about IODOBIS(INDENYL)VANADIUM(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

bis(indenyl)vanadium(II) (101834-69-9) → bis(indenyl)iodovanadium(III) (108150-19-2)

Guidance literature:

With I₂; In toluene; under N2, I2 dissolved in toluene, addn. of (ind)2V, soln. heated just up to boiling; filtered, stored at room temp. for 24h, crystn., filtered, mother liquor stored a few hours at -20°C, then several hours in dry ice, additional crystn., elem. anal.;

Reference yield: 7.0%

bis(indenyl)iodovanadium(III) (108150-19-2) + sodium tetraphenyl borate (143-66-8) → [bis(η5-indenyl)dicarbonylvanadium(III)]tetraphenyl borate*THF

Guidance literature:

With CO; In tetrahydrofuran; THF soln. of complex swirled under CO, addn. of NaBPh4, again swirled under CO; stored overnight at room temp. under CO, elem. anal.;

upstream raw materials:

bis(indenyl)vanadium(II)

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