BIS(INDENYL)VANADIUM(II)

Base Information

Chemical Name:BIS(INDENYL)VANADIUM(II)
CAS No.:101834-69-9
Molecular Formula:C₁₈H₁₄V
Molecular Weight:281.251
Hs Code.:
Mol file:101834-69-9.mol

Synonyms:Bis(h5-indenyl)vanadium

Suppliers and Price of BIS(INDENYL)VANADIUM(II)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BIS(INDENYL)VANADIUM(II) 95.00%
5MG
$ 497.66

Total 4 raw suppliers

Chemical Property of BIS(INDENYL)VANADIUM(II)

Chemical Property:

Melting Point:67 °C (dec.)(lit.)
PSA：0.00000
LogP:4.53160

Purity/Quality:

99% ^*data from raw suppliers

BIS(INDENYL)VANADIUM(II) 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BIS(INDENYL)VANADIUM(II)

There total 2 articles about BIS(INDENYL)VANADIUM(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 20669-47-0
lithium indenide

: 7718-98-1
vanadium(III) chloride

: 101834-69-9
bis(indenyl)vanadium(II)

Guidance literature:: With Zn; In tetrahydrofuran; addn. of VCl3 and Zn in THF to a soln. of indenyl lithium in THF at 0°C, refluxing for 15 h; evapn. to dryness, sublimation in vacuo, recrystn. of the sublimate (toluene-hexane), washing of the crystals, drying at 20°C in vacuo;

Reference yield: 46.0%

: [V₂Cl₃(tetrahydrofuran)₆]₂[Zn₂Cl₆]

: 95-13-6
1-indene

: 101834-69-9
bis(indenyl)vanadium(II)

Guidance literature:: With CH₃Li; In tetrahydrofuran; diethyl ether; under N2, addn. of ether soln. of MeLi to THF soln. of indene (15 min, stirred, gas evolution), addn. of vanadium complex (prepared from refluxing of VCl3 in THF) at room temp., color change; evapn. to dryness, residue sublimed on oil bath up to 180°C for 2.5h, crystn., elem. anal.;

Reference yield: 61.0%

: 101834-69-9
bis(indenyl)vanadium(II)

: 108150-19-2
bis(indenyl)iodovanadium(III)

Guidance literature:: With I₂; In toluene; under N2, I2 dissolved in toluene, addn. of (ind)2V, soln. heated just up to boiling; filtered, stored at room temp. for 24h, crystn., filtered, mother liquor stored a few hours at -20°C, then several hours in dry ice, additional crystn., elem. anal.;