2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

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Chemical Name:2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile
CAS No.:1357114-02-3
Molecular Formula:C₃₇H₄₁N₅O₅S₂
Molecular Weight:699.895
Hs Code.:

2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

Synonyms:2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

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Chemical Property of 2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

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Technology Process of 2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

There total 5 articles about 2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1080662-00-5
4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

: 118739-11-0
2-(1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

: 1357114-02-3
2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2011.12.003

Reference yield:

: 130-00-7
1,8-naphtholactam

: 1357114-02-3
2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / toluene / 4 h / 100 °C

2: sodium hydride / N,N-dimethyl-formamide / 20 °C

With sodium hydride; trichlorophosphate; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2011.12.003

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1357114-02-3
2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; hydroxylamine hydrochloride / 1 h / Reflux

2: p-toluenesulfonyl chloride / 1 h / Heating

3: trichlorophosphate / toluene / 4 h / 100 °C

4: sodium hydride / N,N-dimethyl-formamide / 20 °C

With pyridine; hydroxylamine hydrochloride; sodium hydride; p-toluenesulfonyl chloride; trichlorophosphate; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2011.12.003