4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

Base Information

• Chemical Name: 4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone
• CAS No.: 1080662-00-5
• Molecular Formula: C₂₃H₃₅BrN₂O₅S₂
• Molecular Weight: 563.577

Synonyms:4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

Chemical Property of 4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

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Technology Process of 4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

There total 1 articles about 4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1 ,6-dibromohexane (629-03-8) + (2S)-N-(4-hydroxy-5-methoxy-2-nitrobenzoyl)pyrrolidine-2-carboxaldehyde diethyl thioacetal (140647-02-5) → 4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone (1080662-00-5)

Guidance literature:

With potassium carbonate; In acetone; for 48h; Reflux;

DOI:10.1016/j.ejmech.2010.05.041

Reference yield: 74.0%

4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone (1080662-00-5) + (E)-3-(4-hydroxy-3-methoxyphenyl)-1-[4-(3,4,5-trimethoxybenzoyl)piperazino]-2-propen-1-one (1226909-06-3) → (2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal (1246890-26-5)

Guidance literature:

With potassium carbonate; In acetonitrile; for 12h; Reflux;

DOI:10.1016/j.ejmech.2010.05.041

Reference yield: 64.0%

4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone (1080662-00-5) + 1,8-naphthosultam (603-72-5) → 2-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydro-1λ(6)-naphtho[1,8-cd]isothiazole-1,1-dione (1357114-06-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2011.12.003

upstream raw materials:

1 ,6-dibromohexane

(2S)-N-(4-hydroxy-5-methoxy-2-nitrobenzoyl)pyrrolidine-2-carboxaldehyde diethyl thioacetal

Downstream raw materials:

C₂₃H₃₅N₅O₅S₂

(2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

2-(1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

1-(6-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]hexyl)-1,2-dihydrobenzo[c,d]indol-2-one

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