(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

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Chemical Name:(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one
CAS No.:1401344-85-1
Molecular Formula:C₃₆H₃₅N₇O₅
Molecular Weight:645.718
Hs Code.:

(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

Synonyms:(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

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Chemical Property of (S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

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Technology Process of (S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

There total 15 articles about (S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1401344-84-0
1-((S)-1-hydroxypropan-2-yl)-3-(3-((S)-5-methyl-3-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-2-oxoimidazolidin-1-yl)phenyl)-1-(3-nitrophenyl)urea

: 1401344-85-1
(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; urea; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2cc34791a

Reference yield:

: 645-00-1
m-iodonitrobenzene

: 1401344-85-1
(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

Guidance literature:: Multi-step reaction with 10 steps

1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 36 h / 80 °C / Inert atmosphere

2: dmap; 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: dmap / dichloromethane / 48 h / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C

5: di-isopropyl azodicarboxylate; triphenylphosphine; urea / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6: acetic acid; 5% Pd/C / ethanol; toluene / 3 h / Inert atmosphere

7: sodium hydrogencarbonate / dichloromethane; water / Inert atmosphere

8: dmap / dichloromethane / 48 h / 20 °C / Inert atmosphere

9: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C

10: di-isopropyl azodicarboxylate; triphenylphosphine; urea / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; copper(l) iodide; di-isopropyl azodicarboxylate; 5% Pd/C; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; acetic acid; triphenylphosphine; urea; L-proline; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2cc34791a

Reference yield:

: 1401344-71-5
N-(1-((tert-butyldimethylsilyl)oxy)propan-2-yl)-3-nitroaniline

: 1401344-85-1
(S)-4-methyl-1-(3-((S)-5-methyl-2-oxo-3-phenylimidazolidin-1-yl)phenyl)-3-(3-((S)-4-methyl-3-(3-nitrophenyl)-2-oxoimidazolidin-1-yl)phenyl)imidazolidin-2-one

Guidance literature:: Multi-step reaction with 13 steps

1: dmap / dichloromethane / 48 h / 20 °C

2: tetrabutyl ammonium fluoride; acetic acid / 20 °C / Inert atmosphere

3: di-isopropyl azodicarboxylate; triphenylphosphine; urea / tetrahydrofuran / 0.5 h / 20 °C

4: 5% Pd/C / ethanol / Inert atmosphere

5: sodium hydrogencarbonate / dichloromethane; water / Inert atmosphere

6: dmap / dichloromethane / 48 h / 20 °C / Inert atmosphere

7: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C

8: di-isopropyl azodicarboxylate; triphenylphosphine; urea / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

9: acetic acid; 5% Pd/C / ethanol; toluene / 3 h / Inert atmosphere

10: sodium hydrogencarbonate / dichloromethane; water / Inert atmosphere

11: dmap / dichloromethane / 48 h / 20 °C / Inert atmosphere

12: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C

13: di-isopropyl azodicarboxylate; triphenylphosphine; urea / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With dmap; di-isopropyl azodicarboxylate; 5% Pd/C; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid; triphenylphosphine; urea; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1039/c2cc34791a