6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

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Chemical Name:6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose
CAS No.:870078-06-1
Molecular Formula:C₃₁H₃₃NO₇
Molecular Weight:531.606
Hs Code.:

Synonyms:6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

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Chemical Property of 6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

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Technology Process of 6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

There total 12 articles about 6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 870078-02-7
5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-6,7-dihydroxy-5-deoxy-1,2-O-isopropylidene-β-L-glycero-L-ido-hepto-1,4-furanose

: 870078-06-1
6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

Guidance literature:: With sodium periodate; In acetone; at 15 ℃; for 1h;
DOI:10.1039/b509216g

Reference yield:

: 899431-76-6
3-O-benzyl-1,2-O-isopropylidene-5,6,7-trideoxy-5-(N-benzyl-N-benzoxycarbonylamino)-β-L-ido-6-eno-hepta-1,4-furanose

: 870078-06-1
6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

Guidance literature:: Multi-step reaction with 2 steps

1: NMO; potassium osmate / acetone; H₂O / 12 h / 20 °C

2: 2.20 g / sodium metaperiodate / H₂O / 6 h

With potassium osmate(VI); sodium periodate; N-methyl-2-indolinone; In water; acetone;
DOI:10.1021/jo0601617

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 870078-06-1
6-aldehydo-5-(N-benzyl-N-benzoxycarbonyl)amino-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-β-L-ido-hexo-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium bicarbonate / methanol; H₂O / 3 h / 0 °C

2: NMO; potassium osmate / acetone; H₂O / 12 h / 20 °C

3: 2.20 g / sodium metaperiodate / H₂O / 6 h

With potassium osmate(VI); sodium periodate; N-methyl-2-indolinone; sodium hydrogencarbonate; In methanol; water; acetone;
DOI:10.1021/jo0601617