4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane
CAS No.:1408285-51-7
Molecular Formula:C₁₃H₂₃BO₂SSn
Molecular Weight:372.911
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane

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Chemical Property of 4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane

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Technology Process of 4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane

There total 1 articles about 4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 91509-50-1
C₇H₁₁LiSSn

: 1408285-51-7
4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane

: 37496-13-2
2-(trimethylstannyl)thiophene

: 193978-23-3
2-thiopheneboronic acid pinacol ester

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 13h;
DOI:10.1021/ol302571t

Reference yield: 92.0%

: 591-50-4
iodobenzene

: 1408285-51-7
4,4,5,5-tetramethyl-2-(5-(trimethylstannyl)thiophen-2-yl)-1,3,2-dioxaborolane

: 459409-74-6
4,4,5,5-tetramethyl-2-(5-phenylthiophen-2-yl)-1,3,2-dioxaborolane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromobenzene; In N,N-dimethyl-formamide; at 100 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1021/ol401923j