(S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

Base Information

Chemical Name:(S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate
CAS No.:257876-70-3
Molecular Formula:C₂₆H₄₀O₆SSi
Molecular Weight:508.752
Hs Code.:

Synonyms:(S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

Chemical Property:

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Technology Process of (S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

There total 3 articles about (S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 908338-26-1
Methanesulfonic acid (S)-4,4-diethoxy-2-hydroxymethyl-butyl ester

: 58479-61-1
tert-butylchlorodiphenylsilane

: 257876-70-3
(S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2006.05.033

Reference yield:

: 144461-19-8,134665-24-0
(R)-2-(2,2-diethoxyethyl)-1,3-propanediol monoacetate

: 257876-70-3
(S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.53 g / triethylamine / tetrahydrofuran / 0.42 h / 0 °C

2: 1.31 g / NaOH / dioxane; H₂O / 1 h / 0 °C

3: 2.11 g / imidazole / dimethylformamide / 0 - 20 °C

With 1H-imidazole; sodium hydroxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.05.033

Reference yield:

: 134665-15-9
(S)-2-(acetoxymethyl)-4,4-diethoxybutyl methanesulfonate

: 257876-70-3
(S)-2-(tert-butyldiphenylsilyloxymethyl)-4,4-diethoxybutyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.31 g / NaOH / dioxane; H₂O / 1 h / 0 °C

2: 2.11 g / imidazole / dimethylformamide / 0 - 20 °C

With 1H-imidazole; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.05.033