2,2,2-tribromoethyl cyclohexanecarboxylate

Base Information

• Chemical Name: 2,2,2-tribromoethyl cyclohexanecarboxylate
• CAS No.: 221887-36-1
• Molecular Formula: C₉H₁₃Br₃O₂
• Molecular Weight: 392.913
• Mol file: 221887-36-1.mol

Synonyms:2,2,2-tribromoethyl cyclohexanecarboxylate

Chemical Property of 2,2,2-tribromoethyl cyclohexanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,2,2-tribromoethyl cyclohexanecarboxylate

There total 1 articles about 2,2,2-tribromoethyl cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2,2,2-tribromoethanol (75-80-9) + Cyclohexanecarboxylic acid (98-89-5) → 2,2,2-tribromoethyl cyclohexanecarboxylate (221887-36-1)

Guidance literature:

With dmap; dacarbazine; 4-N,N-dimethylaminopyridine trifluoroacetate; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1021/jo991711m

Reference yield: 88.0%

N-butylamine (109-73-9,85404-21-3) + 2,2,2-tribromoethyl cyclohexanecarboxylate (221887-36-1) → N-Butyl-cyclohexyl carboxamide (128037-34-3)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; triethylamine; In N,N-dimethyl-formamide; at -55 ℃;

DOI:10.1021/jo9823700

Reference yield: 74.0%

2-methoxy-ethanol (109-86-4,95507-80-5) + 2,2,2-tribromoethyl cyclohexanecarboxylate (221887-36-1) → 2-methoxyethyl cyclohexanecarboxylate (36364-14-4)

Guidance literature:

With dmap; tributylphosphine; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1021/jo9823700

upstream raw materials:

2,2,2-tribromoethanol

Cyclohexanecarboxylic acid

Downstream raw materials:

2-methoxyethyl cyclohexanecarboxylate

(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl cyclohexanecarboxylate

N,N-diethylcyclohexanecarboxamide

N-Butyl-cyclohexyl carboxamide