,S^)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

Base Information

Chemical Name:*,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester
CAS No.:161151-77-5
Molecular Formula:C₁₃H₂₀O₅
Molecular Weight:256.299
Hs Code.:

<S-(R<sup>*</sup>,S<sup>*</sup>)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

Synonyms:*,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

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Chemical Property of *,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

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Technology Process of *,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

There total 2 articles about *,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 193468-09-6
[2-Methyl-cyclohex-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

: 686-46-4
methyl 2-acetoxyacrylate

: 161151-77-5
*,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

: 2-Acetoxy-3-(3-methyl-2-oxo-cyclohexyl)-propionic acid methyl ester

Guidance literature:: [2-Methyl-cyclohex-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine; methyl 2-acetoxyacrylate; With hydroquinone; at 20 ℃; for 1.5h;

With acetic acid; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 352695-16-0
(1R_.E)-N-(2-methylcyclohexylidene)-1-phenylethanamine

: 686-46-4
methyl 2-acetoxyacrylate

: 161151-77-5
*,S^*)>-α-(acetyloxy)-1-methyl-2-oxocyclohexanepropanoic acid methyl ester

: 2-Acetoxy-3-(3-methyl-2-oxo-cyclohexyl)-propionic acid methyl ester

Guidance literature:: With acetic acid; hydroquinone; Yield given. Multistep reaction. Yields of byproduct given; 1.) 20 deg C, 90 min, 2.) THF, 20 deg C, 2 h;
DOI:10.1021/jo960140k