(S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Base Information

Chemical Name:(S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester
CAS No.:439912-40-0
Molecular Formula:C₁₅H₁₂F₅NO₄
Molecular Weight:365.257
Hs Code.:

Synonyms:(S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Suppliers and Price of (S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

There total 3 articles about (S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 439912-46-6
Proc-Val-OH

: 439912-40-0
(S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In acetonitrile; at 0 - 20 ℃; for 4h;
DOI:10.1016/S0040-4039(02)00287-3

Reference yield: 87.0%

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 439912-32-0
propargyl pentafluorophenyl carbonate

: 439912-40-0
(S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at -10 - 20 ℃;
DOI:10.1021/ol060494q

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 439912-40-0
(S)-3-Methyl-2-prop-2-ynyloxycarbonylamino-butyric acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaHCO₃ / acetone; H₂O; dimethylformamide / -10 - 20 °C

2: 93 percent / EDC / acetonitrile / 4 h / 0 - 20 °C

With sodium hydrogencarbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0040-4039(02)00287-3