Diethyl malonate

Base Information

• Chemical Name: Diethyl malonate
• CAS No.: 153180-27-9
• Molecular Formula: C₁₆H₂₁NO₅
• Molecular Weight: 307.346

Synonyms:Diethyl malonate

Chemical Property of Diethyl malonate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Diethyl malonate

There total 2 articles about Diethyl malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

diethyl aminomalonate hydrochloride (13433-00-6) + hydrocinnamic acid chloride (645-45-4) → Diethyl malonate (153180-27-9)

Guidance literature:

With potassium carbonate; In dichloromethane; water; 0 deg C to r.t.;

DOI:10.1021/jo00073a040

Reference yield:

dimethyl L-aspartate hydrochloride (32213-95-9) → Diethyl malonate (153180-27-9)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 8h;

DOI:10.1016/j.bmc.2016.11.060

Reference yield:

Diethyl malonate (153180-27-9) → C12H11NO5(2-)*2Na(1+)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 5h;

DOI:10.1016/j.bmc.2016.11.060

upstream raw materials:

diethyl aminomalonate hydrochloride

hydrocinnamic acid chloride

dimethyl L-aspartate hydrochloride

Downstream raw materials:

Methyl 2-(2-phenylethyl)-4-oxazolecarboxylate

Dimethyl <(phenylthio)methyl>malonate

2-Phenethyl-5-phenylsulfanyl-oxazole-4,4-dicarboxylic acid dimethyl ester

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