(E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

Base Information

Chemical Name:(E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate
CAS No.:1579999-09-9
Molecular Formula:C₂₇H₂₂F₆N₄O₄S
Molecular Weight:612.552
Hs Code.:

Synonyms:(E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

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Chemical Property of (E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

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Technology Process of (E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

There total 6 articles about (E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1579999-02-2
(E)-diethyl 5-((3-aminophenyl)diazenyl)isophthalate

: 23165-29-9
3,5-bistrifluoromethylphenylisothiocyanate

: 1579999-09-9
(E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

Guidance literature:: In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol500381c

Reference yield:

: 32338-22-0
2-(3-aminophenyl)isoindoline-1,3-dione

: 1579999-09-9
(E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 24 h / 20 °C

2: hydrazine hydrate / methanol / 5.5 h / 20 °C

3: dichloromethane / 20 °C / Inert atmosphere

With hydrazine hydrate; acetic acid; In methanol; dichloromethane;
DOI:10.1021/ol500381c

Reference yield:

: 106-50-3
1,4-phenylenediamine

: 1579999-09-9
(E)-diethyl 5-((3-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)phenyl)diazenyl)isophthalate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 8 h / Reflux; Dean-Stark

2: acetic acid / 24 h / 20 °C

3: hydrazine hydrate / methanol / 5.5 h / 20 °C

4: dichloromethane / 20 °C / Inert atmosphere

With hydrazine hydrate; acetic acid; In methanol; dichloromethane; toluene;
DOI:10.1021/ol500381c