4-benzyloxy-2,6-dichlorostyrene

Base Information

Chemical Name:4-benzyloxy-2,6-dichlorostyrene
CAS No.:461031-80-1
Molecular Formula:C₁₅H₁₂Cl₂O
Molecular Weight:279.166
Hs Code.:

Synonyms:4-benzyloxy-2,6-dichlorostyrene

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Chemical Property of 4-benzyloxy-2,6-dichlorostyrene

Chemical Property:

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Technology Process of 4-benzyloxy-2,6-dichlorostyrene

There total 5 articles about 4-benzyloxy-2,6-dichlorostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 461031-79-8
4-(benzyloxy)-2,6-dichlorobenzaldehyde

: 461031-80-1
4-benzyloxy-2,6-dichlorostyrene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 1h;
DOI:10.1021/ol026182e

Reference yield:

: 591-35-5
3,5-dichlorophenol

: 461031-80-1
4-benzyloxy-2,6-dichlorostyrene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / imidazole / dimethylformamide / 0.33 h / 20 °C

2.1: sec-BuLi / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C

2.2: 5.7 g / tetrahydrofuran; cyclohexane / 1.5 h / -78 °C

3.1: 7.8 g / K₂CO₃; KI / 16 h / 20 °C

4.1: 85 percent / n-BuLi / tetrahydrofuran; hexane / 1 h / 20 °C

With 1H-imidazole; n-butyllithium; sec.-butyllithium; potassium carbonate; potassium iodide; In tetrahydrofuran; hexane; cyclohexane; N,N-dimethyl-formamide; 4.1: Wittig reaction;
DOI:10.1021/ol026182e

Reference yield:

: 60964-09-2
2,6-dichloro-4-hydroxybenzaldehyde

: 461031-80-1
4-benzyloxy-2,6-dichlorostyrene

Guidance literature:: Multi-step reaction with 2 steps

1: 7.8 g / K₂CO₃; KI / 16 h / 20 °C

2: 85 percent / n-BuLi / tetrahydrofuran; hexane / 1 h / 20 °C

With n-butyllithium; potassium carbonate; potassium iodide; In tetrahydrofuran; hexane; 2: Wittig reaction;
DOI:10.1021/ol026182e