9H-Imidazo[1,2-a]purin-9-one, 5-acetyl-6,7-bis(acetyloxy)-3,5,6,7-tetrahydro-

Base Information

Chemical Name:9H-Imidazo[1,2-a]purin-9-one, 5-acetyl-6,7-bis(acetyloxy)-3,5,6,7-tetrahydro-
CAS No.:107698-70-4
Molecular Formula:C₁₃H₁₃N₅O₆
Molecular Weight:335.276
Hs Code.:
Mol file:107698-70-4.mol

Synonyms:9H-Imidazo[1,2-a]purin-9-one,5-acetyl-6,7-bis(acetyloxy)-1,5,6,7-tetrahydro- (9CI)

Suppliers and Price of 9H-Imidazo[1,2-a]purin-9-one, 5-acetyl-6,7-bis(acetyloxy)-3,5,6,7-tetrahydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 9H-Imidazo[1,2-a]purin-9-one, 5-acetyl-6,7-bis(acetyloxy)-3,5,6,7-tetrahydro-

Chemical Property:

PSA：136.48000
LogP:-0.49800

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9H-Imidazo[1,2-a]purin-9-one, 5-acetyl-6,7-bis(acetyloxy)-3,5,6,7-tetrahydro-

There total 5 articles about 9H-Imidazo[1,2-a]purin-9-one, 5-acetyl-6,7-bis(acetyloxy)-3,5,6,7-tetrahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 105528-80-1
3,5-diacetyl-6,7-diacetoxy-5,6,7,9-tetrahydro-9-oxo(3H-imidazo<1,2-a>-purine)

: 107698-70-4
6,7-diacetoxy-5-acetyl-5,6,7,9-tetrahydro-9-oxo-3H-iminazo[1,2-a]purine

Guidance literature:: With water; In ethanol; at 60 ℃; for 0.5h;

Reference yield: 52.0%

: 108-24-7
acetic anhydride

: 1,N²-glyoxal-N²-acetylguanine

: 107698-70-4
ethanoic acid-5,6,7,9-tetrahydro-5-(1-oxoethyl)-9-oxo-3H-imidazo<1,2-a>purine-6,7-diyl ester

Guidance literature:: In pyridine; for 2h; Ambient temperature;
DOI:10.1002/jhet.5570230264

Reference yield:

: 19962-37-9
N-(6-oxo-6,9-dihydro-1H-purin-2-yl)acetamide

: 107698-70-4
6,7-diacetoxy-5-acetyl-5,6,7,9-tetrahydro-9-oxo-3H-iminazo[1,2-a]purine

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / pyridine / Ambient temperature

2: 70 percent / pyridine / 2 h / Ambient temperature

3: 84 percent / H₂O / ethanol / 0.5 h / 60 °C

With pyridine; water; In ethanol;