7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

Base Information

Chemical Name:7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone
CAS No.:1446491-21-9
Molecular Formula:C₂₄H₂₂ClNO₂
Molecular Weight:391.897
Hs Code.:

Synonyms:7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

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Chemical Property of 7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

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Technology Process of 7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

There total 3 articles about 7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104-88-1
4-chlorobenzaldehyde

: 126-81-8
dimedone

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1446491-21-9
7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

Guidance literature:: With dihydrogen peroxide; ammonium carbonate; In water; at 20 ℃; Green chemistry;
DOI:10.1039/c3gc40441b

Reference yield: 61.0%

: 1107620-86-9
4,6,7,8-tetrahydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(1H)-quinolinone

: 1446491-21-9
7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

Guidance literature:: With sodium acetate; 4-chlorobenzaldehyde; In acetic acid; at 140 ℃; for 8h; Reagent/catalyst;
DOI:10.1002/jhet.1117

Reference yield:

: 6552-68-7
4-chloro-4'-methoxy-chalcone

: 126-81-8
dimedone

: 1446491-21-9
7,8-dihydro-4-(4-chlorophenyl)-2-(4-methoxyphenyl)-7,7-dimethyl-5(6H)-quinolinone

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / ethanol / 0.33 h / Reflux

2: sodium acetate; 4-chlorobenzaldehyde / acetic acid / 8 h / 140 °C

With ammonium acetate; sodium acetate; 4-chlorobenzaldehyde; acetic acid; In ethanol; acetic acid; 2: |Cannizzaro Reaction;
DOI:10.1002/jhet.1117