Technology Process of 2H-Furo[3,2-b]pyrrol-2-one, 4-acetylhexahydro-, (3aR-cis)- (9CI)
There total 27 articles about 2H-Furo[3,2-b]pyrrol-2-one, 4-acetylhexahydro-, (3aR-cis)- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
benzene;
at 80 ℃;
for 0.333333h;
DOI:10.1016/0957-4166(96)00434-X
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 20h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: pyridine
2: NaI / butan-2-one / Heating
3: Hg(OAc)2, NaBH4 / tetrahydrofuran; H2O
4: pyridine
5: H2 / 10percent Pd/C
6: NaOAc / ethanol / Heating
7: pyridine
8: HCl / Heating
10: tributyltin hydride / toluene / Heating
11: 1) aqueous acetic acid, 2) pyridinium chlorochromate / 2) CH2Cl2
With
pyridine; hydrogenchloride; sodium tetrahydroborate; mercury(II) diacetate; hydrogen; tri-n-butyl-tin hydride; sodium acetate; acetic acid; pyridinium chlorochromate; sodium iodide;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; water; toluene; butanone;
