1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

Base Information

Chemical Name:1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene
CAS No.:342808-91-7
Molecular Formula:C₆₃H₆₃N₃O₁₅
Molecular Weight:1102.2
Hs Code.:

Synonyms:1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

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Chemical Property of 1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

Chemical Property:

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Technology Process of 1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

There total 5 articles about 1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 342808-83-7
N-acetyl-2-hydroxy-(3,5-dimethoxyanilino)-acetophenone

: 342808-91-7
1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

Guidance literature:: With potassium carbonate; In acetone; for 24h; Heating;
DOI:10.1016/S0040-4020(01)00053-9

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 342808-91-7
1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / CuBr₂ / CHCl₃; ethyl acetate / Heating

2: 88 percent / NaHCO₃ / ethanol / 2.5 h / Heating

3: 3 h / 20 °C

4: 99 percent / potassium carbonate / acetone / 24 h / Heating

With sodium hydrogencarbonate; potassium carbonate; copper(ll) bromide; In ethanol; chloroform; ethyl acetate; acetone;
DOI:10.1016/S0040-4020(01)00053-9

Reference yield:

: 2491-36-3
2-(2-bromoacetyl)hydroxybenzene

: 342808-91-7
1,3,5-tris(2-(1-acetyl-3,5-dimethoxyphenylaminoacetyl))phenoxymethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NaHCO₃ / ethanol / 2.5 h / Heating

2: 3 h / 20 °C

3: 99 percent / potassium carbonate / acetone / 24 h / Heating

With sodium hydrogencarbonate; potassium carbonate; In ethanol; acetone;
DOI:10.1016/S0040-4020(01)00053-9