(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

Base Information

Chemical Name:(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine
CAS No.:305808-89-3
Molecular Formula:C₂₃H₁₉N₅O₄Se
Molecular Weight:508.395
Hs Code.:

(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N<sup>6</sup>-benzoyladenine

Synonyms:(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

Chemical Property:

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Technology Process of (+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

There total 4 articles about (+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18055-47-5
N-Benzoyl-N,9-bis(trimethylsilyl)adenin

: 194783-62-5
(+/-)-2-benzoyloxymethyl-1,2-oxaselenolane 5-acetate

: 305808-89-3
(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 22h;
DOI:10.1021/jm990113x

Reference yield:

: 4005-49-6
N-benzoyladenine

: 305808-89-3
(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

Guidance literature:: Multi-step reaction with 2 steps

1: (NH₄)2SO₄ / Heating

2: TMSOTf / 1,2-dichloro-ethane / 22 h / 20 °C

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; 1: silylation / 2: Condensation;
DOI:10.1021/jm990113x

Reference yield:

: 194783-61-4
(+/-)-2-benzoyloxymethyl-1,3-oxaselenolan-5-one

: 305808-89-3
(+/-)-α/β-9-(2-benzoyloxymethyl-1,3-oxaselenolan-5-yl)-N⁶-benzoyladenine

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / hexane; tetrahydrofuran / 1 h / -78 °C

2: hexane; tetrahydrofuran / 3 h / 20 °C

3: TMSOTf / 1,2-dichloro-ethane / 22 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; diisobutylaluminium hydride; In tetrahydrofuran; hexane; 1,2-dichloro-ethane; 1: Reduction / 2: Acetylation / 3: Condensation;
DOI:10.1021/jm990113x