ethyl p-cyanobenzenesulphinate

Base Information

• Chemical Name: ethyl p-cyanobenzenesulphinate
• CAS No.: 13165-84-9
• Molecular Formula: C₉H₉NO₂S
• Molecular Weight: 195.242
• Mol file: 13165-84-9.mol

Synonyms:ethyl p-cyanobenzenesulphinate

Chemical Property of ethyl p-cyanobenzenesulphinate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl p-cyanobenzenesulphinate

There total 1 articles about ethyl p-cyanobenzenesulphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 4-cyanobenzene-1-sulfonohydrazide (799797-30-1) → ethyl p-cyanobenzenesulphinate (13165-84-9)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); at 40 ℃; for 20h;

DOI:10.1039/d1nj00390a

Reference yield: 95.0%

indole (120-72-9) + ethyl p-cyanobenzenesulphinate (13165-84-9) → 4-((1H-indol-3-yl)thio)benzonitrile

Guidance literature:

With ammonium iodide; 1,10-Phenanthroline; acetic acid; In 1,4-dioxane; at 100 ℃; for 6h; Sealed tube;

DOI:10.1016/j.tet.2019.130664

Reference yield: 86.0%

N-Methylpyrrole (96-54-8) + ethyl p-cyanobenzenesulphinate (13165-84-9) → 4-((1-methyl-1H-pyrrol-2-yl)thio)benzonitrile

Guidance literature:

With ammonium iodide; 1,10-Phenanthroline; acetic acid; In 1,4-dioxane; at 100 ℃; for 6h; Sealed tube;

DOI:10.1016/j.tet.2019.130664

upstream raw materials:

ethanol

4-cyanobenzene-1-sulfonohydrazide