tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Base Information

Chemical Name:tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate
CAS No.:1112844-81-1
Molecular Formula:C₅₁H₈₁NO₈
Molecular Weight:836.206
Hs Code.:

tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Synonyms:tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

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Chemical Property of tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

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Technology Process of tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

There total 5 articles about tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1112844-45-7
C₄₁H₆₄O₇S

: 108149-63-9,108149-65-1
tert-butyl (4S)-4-(hydroxymethyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate

: 1112844-81-1
tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2008.10.137

Reference yield:

: 1112844-76-4
(1R,2R,5S,7R)-7-(5-(benzyloxy)pentyl)-5-(15-(tert-butyldimethylsilyloxy)pentadecyl)-6,8-dioxabicyclo[3.2.1]octan-2-ol

: 1112844-81-1
tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 1 h / 0 °C

2.1: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 °C

3.2: 0.5 h / 0 °C

4.1: sodium hydride / dimethyl sulfoxide; mineral oil / 16 h / 20 °C

With sodium hydride; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2012.12.045

Reference yield:

: 1112844-78-6
(15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)(tert-butyl)dimethylsilane

: 1112844-81-1
tert-butyl 4-((15-((1R,2R,5S,7R)-2-(benzyloxy)-7-(5-(benzyloxy)pentyl)-6,8-dioxabicyclo[3.2.1]octan-5-yl)pentadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C

2.2: 0.5 h / 0 °C

3.1: sodium hydride / dimethyl sulfoxide; mineral oil / 16 h / 20 °C

With sodium hydride; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1016/j.tet.2012.12.045