2-hexahydropyrimidine

Base Information

• Chemical Name: 2-hexahydropyrimidine
• CAS No.: 138963-32-3
• Molecular Formula: C₁₈H₁₆N₄O₅
• Molecular Weight: 368.349

Synonyms:2-hexahydropyrimidine

Chemical Property of 2-hexahydropyrimidine

Chemical Property:

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Technology Process of 2-hexahydropyrimidine

There total 4 articles about 2-hexahydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + 1-phenyl-2-(tetrahydropyrimidin-2(1H)-ylidene)ethan-1-one (82100-30-9) → 2-hexahydropyrimidine (138963-32-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

Reference yield: 53.0%

1-phenyl-2-(tetrahydropyrimidin-2(1H)-ylidene)ethan-1-one (82100-30-9) + 1-chloro-2,4-dinitro-benzene (97-00-7) → 2-hexahydropyrimidine (138963-32-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

Reference yield: 32.0%

2,4-dinitrobromobenzene (584-48-5) + 1-phenyl-2-(tetrahydropyrimidin-2(1H)-ylidene)ethan-1-one (82100-30-9) → 2-hexahydropyrimidine (138963-32-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

upstream raw materials:

2,4-dinitrobromobenzene

1-phenyl-2-(tetrahydropyrimidin-2(1H)-ylidene)ethan-1-one

1-iodo-2,4-dinitrobenzene

2,4-Dinitrofluorobenzene

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