methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

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Chemical Name:methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate
CAS No.:1356599-84-2
Molecular Formula:C₂₆H₂₈N₂O₄
Molecular Weight:432.519
Hs Code.:

Synonyms:methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

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Chemical Property of methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

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Technology Process of methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

There total 3 articles about methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.4%

: 35418-07-6
methyl 3-(4-aminophenyl)propionate

: 1356599-82-0
4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzaldehyde

: 1356599-84-2
methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

Guidance literature:: methyl 3-(4-aminophenyl)propionate; 4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzaldehyde; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 2.25h;

With water; sodium hydrogencarbonate; In 1,2-dichloro-ethane; at 20 ℃;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356599-84-2
methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium acetate; acetic acid / 0.08 h / 20 °C

1.2: 3 h / 20 - 80 °C

2.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

2.2: 5 h / 20 - 80 °C

3.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 2.25 h / 0 - 20 °C

3.2: 20 °C

With sodium acetate; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 142533-52-6
(Z)-2-bromo-1-phenylethanone O-methyl oxime

: 1356599-84-2
methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)amino]phenyl}propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

1.2: 5 h / 20 - 80 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 2.25 h / 0 - 20 °C

2.2: 20 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; In 1,2-dichloro-ethane; acetonitrile;