N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

Base Information

Chemical Name:N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide
CAS No.:329966-95-2
Molecular Formula:C₂₂H₂₆N₂O₄
Molecular Weight:382.459
Hs Code.:

Synonyms:N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

Chemical Property:

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Technology Process of N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

There total 6 articles about N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 329966-94-1
(S)-methyl 7-(tert-butoxycarbonylamino)-8-oxo-8-(phenylamino)octanoate

: 65-85-0,8013-63-6
benzoic acid

: 329966-95-2
N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

Guidance literature:: (S)-methyl 7-(tert-butoxycarbonylamino)-8-oxo-8-(phenylamino)octanoate; With trifluoroacetic acid; In dichloromethane; for 12.5h;

benzoic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: N-butoxycarbonyl-2-L-aminosuberic acid ω-methyl ester

: 329966-95-2
N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

Guidance literature:: Multi-step reaction with 3 steps

1: EDC; HOBt / dimethylformamide

2: TFA / CH₂Cl₂

3: NMM / dimethylformamide

With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.04.089

Reference yield:

: 329966-94-1
(S)-methyl 7-(tert-butoxycarbonylamino)-8-oxo-8-(phenylamino)octanoate

: 329966-95-2
N-benzoyl-ω-methyl-(L)-α-aminosuberateanilide

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂

2: NMM / dimethylformamide

With 4-methyl-morpholine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.04.089