benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

Base Information

Chemical Name:benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate
CAS No.:1297549-08-6
Molecular Formula:C₃₄H₃₄ClNO₅
Molecular Weight:572.101
Hs Code.:

Synonyms:benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

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Chemical Property of benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

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Technology Process of benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

There total 5 articles about benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1242160-03-7
benzyl 2-(oxetan-3-ylidene)acetate

: 1297549-07-5
{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}boronic acid

: 1297549-08-6
benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

Guidance literature:: With potassium hydroxide; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In 1,4-dioxane; water; at 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1297549-08-6
benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: n-butyllithium / hexane; diethyl ether; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 3.25 h / -78 - 20 °C

2.3: Cooling with ice

3.1: potassium hydroxide / chloro(1,5-cyclooctadiene)rhodium(I) dimer / 1,4-dioxane; water / 4 h / 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; potassium hydroxide; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; water; mineral oil;

Reference yield:

: 15097-38-8
(carbobenzyloxymethylene)triphenylphosphorane

: 1297549-08-6
benzyl (3-{3-[bis(4-methoxybenzyl)amino]-4-chlorophenyl}oxetan-3-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium hydroxide / chloro(1,5-cyclooctadiene)rhodium(I) dimer / 1,4-dioxane; water / 4 h / 20 °C / Inert atmosphere

With potassium hydroxide; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In 1,4-dioxane; dichloromethane; water;