1-Hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptan-2-one

Base Information

Chemical Name:1-Hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptan-2-one
CAS No.:107243-99-2
Molecular Formula:C₁₀H₁₆O₂
Molecular Weight:168.236
Hs Code.:2914400090
Mol file:107243-99-2.mol

Synonyms:Bicyclo[2.2.1]heptan-2-one,1-(hydroxymethyl)-7,7-dimethyl-, (1R)-; (1R)-10-Hydroxycamphor; D-10-Hydroxycamphor

Suppliers and Price of 1-Hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-Hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptan-2-one

Chemical Property:

PSA：37.30000
LogP:1.37410

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptan-2-one

There total 16 articles about 1-Hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 159928-72-0
(1R)-2-(N-2-pyridylmethyl)iminobornane

: 1925-51-5,107243-99-2
(1R,4R)-1-hydroxymethyl-7,7-dimethyl-bicyclo[2.2.1]heptan-2-one

Guidance literature:: (1R)-2-(N-2-pyridylmethyl)iminobornane; With tetrakis(actonitrile)copper(I) hexafluorophosphate; oxygen; sodium L-ascorbate; In methanol; acetone; at 20 - 50 ℃; for 6.08333h;

With water; ethylene diamine tetraacetic acid tetrasodium salt; In methanol; ethyl acetate; acetone; at 20 ℃; for 15h; pH=Ca. 10; Reagent/catalyst; chemoselective reaction;
DOI:10.1021/jacs.5b09463

Reference yield: 92.0%

: 1925-53-7,108266-83-7
(1R,4R)-10-acetoxycamphor

: 1925-51-5,107243-99-2
(1R,4R)-1-hydroxymethyl-7,7-dimethyl-bicyclo[2.2.1]heptan-2-one

Guidance literature:: With potassium hydroxide; In methanol; at 65 ℃; for 6h;
DOI:10.1002/ejoc.201200075

Reference yield: 78.0%

: 22780-14-9
(1R)-3,3-dimethyl-2-methylenenorbornan-1-ol

: 1925-51-5,107243-99-2
(1R,4R)-1-hydroxymethyl-7,7-dimethyl-bicyclo[2.2.1]heptan-2-one

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/S0957-4166(00)00416-X DOI:10.1021/jo026566i