N⁶-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine

Base Information

• Chemical Name: N⁶-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine
• CAS No.: 96760-66-6
• Molecular Formula: C₂₇H₂₈N₆O₇
• Molecular Weight: 548.555

Synonyms:N⁶-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine

Chemical Property of N⁶-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine

Chemical Property:

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Technology Process of N⁶-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine

There total 3 articles about N⁶-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

phenyl>acetic acid (96760-57-5) + methyl 2-(4-aminophenyl)acetate hydrochloride (83528-16-9) → N6-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine (96760-66-6)

Guidance literature:

With N-ethylmorpholine;; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 2h; Ambient temperature;

DOI:10.1021/jm00147a038

Reference yield:

6-Chloropurine riboside (2004-06-0) → N6-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine (96760-66-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / triethylamine / ethanol; H₂O / 72 h / 80 °C

2: 66 percent / EDAC, 1-hydroxybenzotriazole, N-ethylmorpholine / dimethylformamide / 2 h / Ambient temperature

With N-ethylmorpholine;; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1021/jm00147a038

Reference yield:

methyl p-aminophenylacetate (39552-81-3) + phenyl>acetic acid (96760-57-5) → N6-<4-<<<<4-<<(Methyloxy)carbonyl>methyl>phenyl>amino>carbonyl>methyl>phenyl>adenosine (96760-66-6)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;

upstream raw materials:

methyl p-aminophenylacetate

phenyl>acetic acid

methyl 2-(4-aminophenyl)acetate hydrochloride

6-Chloropurine riboside

Downstream raw materials:

2-{4-[9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-9H-purin-6-ylamino]-phenyl}-N-(4-hydrazinocarbonylmethyl-phenyl)-acetamide

N-(4-(2-((4-(2-((2-aminoethyl)amino)-2-oxoethyl)phenyl)amino)-2-oxoethyl)phenyl)adenosine

N-(2-{2-[4-(2-{4-[9-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-9H-purin-6-ylamino]-phenyl}-acetylamino)-phenyl]-acetylamino}-ethyl)-3-(4-hydroxy-phenyl)-propionamide

N-Acetyl-ADAC

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