3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

Base Information

Chemical Name:3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione
CAS No.:902757-40-8
Molecular Formula:C₁₅H₁₉NO₂S₂
Molecular Weight:309.453
Hs Code.:

Synonyms:3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

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Chemical Property of 3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

Chemical Property:

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Technology Process of 3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

There total 2 articles about 3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71432-55-8
2-tert-butyl-1,3-diisopropylisourea

: 529477-58-5
N-(hydroxy)-5-(p-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 902757-40-8
3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 1293965-57-7
2-(2-methylpropyl-2-sulfanyl)-5-(4-methoxyphenyl)-4-methylthiazole N-oxide

Guidance literature:: In dichloromethane; at 24 ℃; for 1.5h;
DOI:10.1016/j.tet.2010.12.071

Reference yield:

: 507-20-0
tertiary butyl chloride

: N-(hydroxy)-5-(p-methoxyphenyl)-4-(methyl)thiazole-2(3H)-thione tetraethylammonium salt

: 902757-40-8
3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

Guidance literature:: In dichloromethane; at 20 ℃; for 24h;
DOI:10.1039/b603480b

Reference yield: 84.0%

: 902757-40-8
3-(2-methylprop-2-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 75-62-7
Bromotrichloromethane

: 498-66-8
norbornene

: 2-exo-3-exo-2-bromo-3-trichloromethylbicyclo[2.2.1]heptane

: 2-exo-3-exo-2-bromo-3-(2-methylprop-2-oxy)-bicyclo[2.2.1]heptane

: 2-endo-3-exo-2-bromo-3-(2-methylprop-2-oxy)-bicyclo[2.2.1]heptane

: 2-(3-chlorobicyclo[2.2.1]hept-2-ylsulfanyl)-5-(4-methoxyphenyl)-4-methylthiazole

: 19640-08-5,23757-01-9,25612-40-2,62742-49-8
endo-3-bromo-exo-2-trichloromethylbicyclo<2.2.1>heptane

Guidance literature:: In α,α,α-trifluorotoluene; at 25 ℃; for 0.666667h; optical yield given as %de; diastereoselective reaction; Photolysis;
DOI:10.1016/j.tet.2010.12.071