Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

Base Information

Chemical Name:Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)
CAS No.:127570-42-7
Molecular Formula:C₃₉H₄₀Co₂O₄P₂Si₂
Molecular Weight:808.849
Hs Code.:

Synonyms:Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

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Chemical Property of Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

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Technology Process of Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

There total 4 articles about Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 625857-56-9
Co4(μ-CO)3(CO)7(μ-dppm)

: 4526-07-2
1,4-bis(trimethylsilyl)-1,3-butadiyne

: 127570-42-7
Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

: [Co4(CO)8(μ-dppm)(μ4-η2-(methyl)3SiC2CCSi(methyl)3]2

Guidance literature:: In dichloromethane; N2; heating of dichloromethane soln. of Co complex and 1,4-bis(trimethylsilyl)butadiyne at 55°C for 3 d; solvent removal, chromy. (TLC, hexane/CH2Cl2 50/50); elem. anal.;
DOI:10.1021/om030327j

Reference yield: 9.0%

: 411233-94-8
Co2(CO)6(μ-((C6H5)2PCH2P(C6H5)2))

: 558456-33-0
1,6-bis(trimethylsilyl)-3-(trimethylsilylethynyl)hex-3-ene-1,5-diyne

: 558456-35-2
[(Co2(CO)4(μ-dppm))2(μ,η2-(Me3SiC2C(H)=C(C.ident.CSiMe3)2)]

: 127570-42-7
Co2(CO)4(μ-dppm)(μ-η2-Me3SiC2CCSiMe3)

: 558456-37-4
[Co2(CO)4(μ-dppm)(μ,η2-Me3SiC2C(C.ident.CSiMe3)=C(C.ident.CSiMe3)2)]

Guidance literature:: With C₂(CCSi(CH₃)3)4; (CCl)2(CCSi(CH₃)3)2; CCl₂C(CCSi(CH₃)3)2; In benzene; (N2); dissolving cobalt cluster and a mixt. of alkynes in C6H6, refluxing with sytirring for 15 min, addn. of cobalt cluster, refluxing for 20 min; evapn., preparative thin layer chromy. (CH2Cl2/hexane 20:80), crystn. (CH2Cl2/MeOH); elem. anal.;
DOI:10.1016/S0022-328X(02)02191-5