4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Base Information

Chemical Name:4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde
CAS No.:1253733-51-5
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:

Synonyms:4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Suppliers and Price of 4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

There total 5 articles about 4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1253733-50-4
3-(4-hydroxymethyl-2,6-dimethoxyphenyl)propan-1-ol

: 1253733-51-5
4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Guidance literature:: With manganese(IV) oxide; In ethanol; for 16h; Reflux;

Reference yield:

: 134-96-3
syringic aldehyde

: 1253733-51-5
4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 16 h / 0 - 20 °C

2.1: 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate / N,N-dimethyl-formamide / 16 h / 115 °C / Inert atmosphere

3.1: methanol; sodium hydroxide / 16 h / 20 °C

4.1: palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine / ethanol / 16 h / 750.08 Torr

4.2: 3 h / Reflux

5.1: manganese(IV) oxide / ethanol / 16 h / Reflux

With pyridine; methanol; manganese(IV) oxide; palladium 10% on activated carbon; 1,3-bis-(diphenylphosphino)propane; hydrogen; palladium diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 137898-19-2
trifluoromethanesulfonic acid 4-formyl-2,6-dimethoxyphenyl ester

: 1253733-51-5
4-(3-hydroxy-propyl)-3,5-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate / N,N-dimethyl-formamide / 16 h / 115 °C / Inert atmosphere

2.1: methanol; sodium hydroxide / 16 h / 20 °C

3.1: palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine / ethanol / 16 h / 750.08 Torr

3.2: 3 h / Reflux

4.1: manganese(IV) oxide / ethanol / 16 h / Reflux

With methanol; manganese(IV) oxide; palladium 10% on activated carbon; 1,3-bis-(diphenylphosphino)propane; hydrogen; palladium diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;