2,3-difluoro-4-pentylphenylmethanol

Base Information

Chemical Name:2,3-difluoro-4-pentylphenylmethanol
CAS No.:538341-94-5
Molecular Formula:C₁₂H₁₆F₂O
Molecular Weight:214.255
Hs Code.:

Synonyms:2,3-difluoro-4-pentylphenylmethanol

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Chemical Property of 2,3-difluoro-4-pentylphenylmethanol

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Technology Process of 2,3-difluoro-4-pentylphenylmethanol

There total 1 articles about 2,3-difluoro-4-pentylphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 126163-54-0
1,2-difluoro-3-pentylbenzene

: 538341-94-5
2,3-difluoro-4-pentylphenylmethanol

Guidance literature:: 1,2-difluoro-3-pentylbenzene; With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane; at -100 ℃; for 1.5h;

formaldehyd; In tetrahydrofuran; hexane; at -100 - 20 ℃;
DOI:10.1039/b210765a

Reference yield: 77.0%

: 538341-94-5
2,3-difluoro-4-pentylphenylmethanol

: 538341-96-7
2,3-difluoro-4-pentylphenylchloromethane

Guidance literature:: With hydrogenchloride; zinc(II) chloride; for 4h; Heating;
DOI:10.1039/b210765a

Reference yield:

: 538341-94-5
2,3-difluoro-4-pentylphenylmethanol

: 5-(2,3-difluoro-4-pentyl-phenyl)-2-(4-ethoxy-2,3-difluoro-phenyl)-[1,3]dioxane

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / ZnCl₂; aq. HCl / 4 h / Heating

2: 86 percent / ethanol; H₂O / 4 h / Heating

3: 71 percent / H₂SO₄ / 6 h / 95 °C

4: NaOMe / toluene / 4 h / 45 °C

5: 4.5 g / NaBH₄ / ethanol / 4 h / 55 °C

6: p-toluenesulfonic acid / toluene / Heating

With hydrogenchloride; sodium tetrahydroborate; sulfuric acid; sodium methylate; toluene-4-sulfonic acid; zinc(II) chloride; In ethanol; water; toluene;
DOI:10.1039/b210765a