Benzaldehyde, 2-ethyl-6-methyl- (9CI)

Base Information

• Chemical Name: Benzaldehyde, 2-ethyl-6-methyl- (9CI)
• CAS No.: 106976-44-7
• Molecular Formula: C10H12 O
• Molecular Weight: 148.205
• Hs Code.: 2912299000
• Mol file: 106976-44-7.mol

Synonyms:2-Ethyl-6-methylbenzaldehyde

Chemical Property of Benzaldehyde, 2-ethyl-6-methyl- (9CI)

Chemical Property:

• PSA: 17.07000
• LogP: 2.36990
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

2-Ethyl-6-methylbenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 2-ethyl-6-methyl- (9CI)

There total 6 articles about Benzaldehyde, 2-ethyl-6-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-ethyl-6-methyl(hydroxymethyl)benzene (106976-43-6) → 2-ethyl-6-methylbenzaldehyde (106976-44-7)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1021/jo00383a006

Reference yield: 83.0%

butyl-[1-(2-chloro-6-methyl-phenyl)-meth-(E)-ylidene]-amine (945408-08-2) + ethylmagnesium chloride (2386-64-3) → 2-ethyl-6-methylbenzaldehyde (106976-44-7)

Guidance literature:

manganese(ll) chloride; In tetrahydrofuran; diethyl ether; at 0 - 50 ℃; for 1.5h;

Reference yield:

2-ethyl-6-methyl-bromobenzene (65232-55-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2-ethyl-6-methylbenzaldehyde (106976-44-7)

Guidance literature:

2-ethyl-6-methyl-bromobenzene; With magnesium; iodine; In tetrahydrofuran; at 25 - 40 ℃; for 1.66667h;

N,N-dimethyl-formamide; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

upstream raw materials:

2-ethyl-6-methyl(hydroxymethyl)benzene

2-ethyl-6-methyl-bromobenzene

2-ethyl-6-methylbenzoic acid

2-ethyl-6-methylcarbomethoxybenzene

Downstream raw materials:

Bis-(2-ethyl-6-methyl-phenyl)-methanol

2-<2-Ethyl-6-methyl-phenyl>-indan-1,3-dion

bis(2-ethyl-6-methylphenyl)methane

1,1-bis(2-ethyl-6-methylphenyl)ethane

Refernces

• 1、 -. "DERIVATIVES OF IMIDAZO (1,2-A) PYRIDINE USEFUL AS MEDICAMENTS FOR TREATING GASTROINTESTINAL DISEASES". Page/Page column 20-21. . Retrieved 2010/11/24.