Benzene, 1,1'-methylenebis[2-ethyl-6-methyl-

Base Information

Chemical Name:Benzene, 1,1'-methylenebis[2-ethyl-6-methyl-
CAS No.:106976-39-0
Molecular Formula:C19H24
Molecular Weight:252.4
Hs Code.:
Mol file:106976-39-0.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1,1'-methylenebis[2-ethyl-6-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, 1,1'-methylenebis[2-ethyl-6-methyl-

There total 6 articles about Benzene, 1,1'-methylenebis[2-ethyl-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 106976-41-4
Bis-(2-ethyl-6-methyl-phenyl)-methanol

: 106976-39-0
bis(2-ethyl-6-methylphenyl)methane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 24h; Ambient temperature;
DOI:10.1021/jo00383a006

Reference yield:

: 106976-43-6
2-ethyl-6-methyl(hydroxymethyl)benzene

: 106976-39-0
bis(2-ethyl-6-methylphenyl)methane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) Mg / 1.) ether, reflux, 5 h, 2.) ether, reflux, 2 h

3: 64 percent / H₂ / 10percent palladium on coal / ethanol / 24 h / Ambient temperature

With hydrogen; magnesium; pyridinium chlorochromate; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo00383a006

Reference yield:

: 65232-55-5
2-ethyl-6-methyl-bromobenzene

: 106976-39-0
bis(2-ethyl-6-methylphenyl)methane

Guidance literature:: Multi-step reaction with 6 steps

2: 98 percent / diethyl ether / Ambient temperature

3: 75 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating

4: 98 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h / Ambient temperature

5: 1.) Mg / 1.) ether, reflux, 5 h, 2.) ether, reflux, 2 h

6: 64 percent / H₂ / 10percent palladium on coal / ethanol / 24 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; magnesium; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo00383a006