N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

Base Information

Chemical Name:N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide
CAS No.:1448791-48-7
Molecular Formula:C₂₀H₂₄N₆O₅S
Molecular Weight:460.514
Hs Code.:

Synonyms:N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

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Chemical Property of N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

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Technology Process of N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

There total 5 articles about N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₂N₆O₃

: 124-63-0
methanesulfonyl chloride

: 1448791-48-7
N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

Guidance literature:: With pyridine; at 50 ℃; for 5h;
DOI:10.1016/j.bmcl.2013.06.038

Reference yield:

: 1049978-48-4,685113-70-6
3,4,5-trimethoxyphenylbiguanide

: 1448791-48-7
N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium methylate / tetrahydrofuran / 0.33 h / 70 °C / Microwave irradiation

2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; palladium diacetate; caesium carbonate / 1,4-dioxane / 150 °C / Microwave irradiation

3: 2-amino-N-ethylbenzamide; palladium 10% on activated carbon / methanol / Inert atmosphere

4: pyridine / 5 h / 50 °C

With pyridine; palladium 10% on activated carbon; 2-amino-N-ethylbenzamide; sodium methylate; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1016/j.bmcl.2013.06.038

Reference yield:

: 1374227-41-4
6-methyl-N-(2-nitrophenyl)-N'-(3,4,5-trimethoxyphenyl)-1,3,5-triazine-2,4-diamine

: 1448791-48-7
N-(2-(4-methyl-6-(3,4,5-trimethoxyphnylamino)-1,3,5-triazin-2-ylamino)phenyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2-amino-N-ethylbenzamide; palladium 10% on activated carbon / methanol / Inert atmosphere

2: pyridine / 5 h / 50 °C

With pyridine; palladium 10% on activated carbon; 2-amino-N-ethylbenzamide; In methanol;
DOI:10.1016/j.bmcl.2013.06.038