α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct

Base Information

• Chemical Name: α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct
• CAS No.: 120789-78-8
• Molecular Formula: C₁₆H₁₆O₅S
• Molecular Weight: 320.366
• Mol file: 120789-78-8.mol

Synonyms:α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct

Chemical Property of α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct

There total 2 articles about α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

α-(phenylsulfonyl)maleic anhydride (120789-76-6) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct (120789-78-8)

Guidance literature:

In acetone; at 28 ℃; for 0.0166667h;

DOI:10.1021/jo00273a015

Reference yield:

α-(phenylthio)maleic anhydride (84649-32-1) → α-(phenylsulfonyl)maleic anhydride-2,3-dimethyl-1,3-butadiene adduct (120789-78-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / Heating

2: 95 percent / acetone / 0.02 h / 28 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetone;

DOI:10.1021/jo00273a015

upstream raw materials:

α-(phenylsulfonyl)maleic anhydride

2,3-dimethyl-buta-1,3-diene

α-(phenylthio)maleic anhydride