7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

Base Information

Chemical Name:7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate
CAS No.:1447673-35-9
Molecular Formula:C₁₁H₈O₃*C₂₈H₃₃N₃O₂
Molecular Weight:631.772
Hs Code.:

Synonyms:7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

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Chemical Property of 7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

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Technology Process of 7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

There total 7 articles about 7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356331-63-9
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid

: 86-48-6
1-hydroxy-2-naphthoic acid

: 1447673-35-9
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

Guidance literature:: In acetonitrile; at 20 ℃; Solvent; Temperature;

Reference yield:

: 2,3-di-p-tolylpyrido[2,3-b]pyrazine acetate

: 1447673-35-9
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen; triethylamine / tetrahydrofuran; ethanol / 168 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 0.17 h / 20 °C

2.2: 20 - 40 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 7.5 h / 50 °C

4.1: acetonitrile / 20 °C

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 1356332-88-1
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid ethyl ester

: 1447673-35-9
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid xinafoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate / tetrahydrofuran; water / 7.5 h / 50 °C

2: acetonitrile / 20 °C

With lithium hydroxide monohydrate; In tetrahydrofuran; water; acetonitrile;