4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

Base Information

Chemical Name:4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether
CAS No.:158263-47-9
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

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Chemical Property of 4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

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Technology Process of 4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

There total 5 articles about 4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 22666-84-8
4-hydroxybenzaldehyde sodium salt

: 158263-46-8
4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)-N-chloroacetanilide

: 158263-47-9
4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

Guidance literature:: In N,N-dimethyl-formamide; for 8h; Heating;
DOI:10.1007/BF00531400

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 158263-47-9
4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / potash / butan-2-one / 24 h / Heating

2: 73 percent / KOH / ethanol / 6 h / Heating

3: 83 percent / diethyl ether

4: 70 percent / dimethylformamide / 8 h / Heating

With potassium hydroxide; potassium carbonate; In diethyl ether; ethanol; N,N-dimethyl-formamide; butanone;
DOI:10.1007/BF00531400

Reference yield:

: 79862-81-0
3,4-dibromo-4-methyltetrahydropyran

: 158263-47-9
4'-formylphenyl-4-(3,6-dihydro-4-methyl-2H-pyran-3-yl-hydroxy)phenylaminocarbonylmethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / potash / butan-2-one / 24 h / Heating

2: 73 percent / KOH / ethanol / 6 h / Heating

3: 83 percent / diethyl ether

4: 70 percent / dimethylformamide / 8 h / Heating

With potassium hydroxide; potassium carbonate; In diethyl ether; ethanol; N,N-dimethyl-formamide; butanone;
DOI:10.1007/BF00531400