(S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

Base Information

Chemical Name:(S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate
CAS No.:1448621-32-6
Molecular Formula:C₁₇H₂₃NO₃Se
Molecular Weight:368.335
Hs Code.:

Synonyms:(S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

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Chemical Property of (S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

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Technology Process of (S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

There total 6 articles about (S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1448621-19-9
(S)-5-(p-tolylselanylmethyl)pyrrolidin-2-one

: 1448621-32-6
(S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c3ob40879e

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1448621-32-6
(S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 3 h / 0 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.17 h / 20 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

3.1: triethylamine; dmap / dichloromethane / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/c3ob40879e

Reference yield:

: 56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
L-glutamic acid

: 1448621-32-6
(S)-tert-butyl 2-oxo-5-(p-tolylselanylmethyl)pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: water / 63 h / Reflux

2.1: thionyl chloride / 48 h / 20 °C

3.1: sodium tetrahydroborate; ethanol / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 3 h / 0 °C

5.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.17 h / 20 °C / Inert atmosphere

5.2: 24 h / 20 °C / Inert atmosphere

6.1: triethylamine; dmap / dichloromethane / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; thionyl chloride; ethanol; water; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/c3ob40879e