1-Bromo-3-iodo-2-methoxybenzene, 2-Bromo-6-iodophenyl methyl ether

Base Information

• Chemical Name: 1-Bromo-3-iodo-2-methoxybenzene, 2-Bromo-6-iodophenyl methyl ether
• CAS No.: 860584-68-5
• Molecular Formula: C₇H₆BrIO
• Molecular Weight: 312.933
• Hs Code.: 2909309090
• Mol file: 860584-68-5.mol

Synonyms:2-bromo-6-iodoanisole

Chemical Property of 1-Bromo-3-iodo-2-methoxybenzene, 2-Bromo-6-iodophenyl methyl ether

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

2-Bromo-6-iodoanisole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Bromo-3-iodo-2-methoxybenzene, 2-Bromo-6-iodophenyl methyl ether

There total 4 articles about 1-Bromo-3-iodo-2-methoxybenzene, 2-Bromo-6-iodophenyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-2-methoxyphenylamine (116557-46-1) → 2-bromo-6-iodoanisole (860584-68-5)

Guidance literature:

With sulfuric acid; Diazotization_.Behandlung der Diazoniumsalz-Loesung mit KI;

DOI:10.1021/ja01323a043

Reference yield:

2-bromoanisole (578-57-4) → 2-bromo-6-iodoanisole (860584-68-5)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid anhydride; HNO₃

2: aqueous hydrochloric acid; iron

3: aqueous H₂SO₄ / Diazotization_.Behandlung der Diazoniumsalz-Loesung mit KI

With hydrogenchloride; sulfuric acid; nitric acid; acetic anhydride; iron;

DOI:10.1021/ja01323a043

Reference yield:

2-bromo-6-nitro-phenol (13073-25-1) → 2-bromo-6-iodoanisole (860584-68-5)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃; xylene

2: aqueous hydrochloric acid; iron

3: aqueous H₂SO₄ / Diazotization_.Behandlung der Diazoniumsalz-Loesung mit KI

With hydrogenchloride; sulfuric acid; iron; potassium carbonate; xylene;

DOI:10.1021/ja01323a043

upstream raw materials:

3-bromo-2-methoxyphenylamine

2-bromoanisole

2-bromo-6-nitro-phenol

2-bromo-6-nitrophenyl methyl ether