2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine

Base Information

• Chemical Name: 2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine
• CAS No.: 119294-21-2
• Molecular Formula: C₂₁H₂₅Cl₆N₃O
• Molecular Weight: 548.167

Synonyms:2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine

Chemical Property of 2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine

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Technology Process of 2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine

There total 1 articles about 2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

3-(3,5-di-tert-butyl-4-hydroxy-phenyl)-propionitrile (29027-77-8) + trichloroacetonitrile (545-06-2) → 2,4,6-tris(trichloromethyl)-s-triazine (6542-67-2) + 2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine (119294-21-2)

Guidance literature:

With hydrogenchloride; aluminum tri-bromide; In diethyl ether; a) 20 deg C, 12 h, b) 100 deg C, 2 h;

DOI:10.1007/BF01165016

Reference yield: 83.0%

2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine (119294-21-2) → 2,6-Di-tert-butyl-4-[2-(4,6-dimethyl-[1,3,5]triazin-2-yl)-ethyl]-phenol

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Heating;

DOI:10.1007/BF01166336

Reference yield: 80.0%

γ-(4-hydroxy-3,5-di-tert-butylphenyl)propylamine (19510-14-6) + 2,4-bis(trichloromethyl)-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine (119294-21-2) → C37H53Cl3N4O2 (119294-26-7)

Guidance literature:

In 1,4-dioxane; at 30 - 35 ℃; for 4h;

DOI:10.1007/BF00755699

upstream raw materials:

3-(3,5-di-tert-butyl-4-hydroxy-phenyl)-propionitrile

trichloroacetonitrile

Downstream raw materials:

C₃₇H₅₃Cl₃N₄O₂

C₅₃H₈₁N₅O₃

2-amino-4-<γ-(4-hydroxy-3,5-di-tert-butylphenyl)propylamino>-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine

2-dimethylamino-4-<γ-(4-hydroxy-3,5-di-tert-butylphenyl)propylamino>-6-<β-(4-hydroxy-3,5-di-tert-butylphenyl)ethyl>-sym-triazine

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