methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

Base Information

Chemical Name:methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside
CAS No.:258286-63-4
Molecular Formula:C₄₆H₅₅N₉O₁₆
Molecular Weight:989.993
Hs Code.:

methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

Synonyms:methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

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Chemical Property of methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

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Technology Process of methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

There total 2 articles about methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 75-36-5
acetyl chloride

: 258286-62-3
methyl O-(2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

: 258286-63-4
methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

Guidance literature:: methyl O-(2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside; With di(n-butyl)tin oxide; In acetonitrile; at 80 ℃; for 14h;

acetyl chloride; In acetonitrile; at 20 ℃;
DOI:10.1016/s0040-4020(99)00869-8

Reference yield:

: 258286-60-1
methyl O-(2-azido-6-O-benzyl-2-desoxy-3,4-O-isopropylidene-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

: 258286-63-4
methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 84 percent / aq. AcOH / 0.17 h / 80 °C

2.1: nBu₂SnO / acetonitrile / 14 h / 80 °C

2.2: 97 percent / acetonitrile / 20 °C

With di(n-butyl)tin oxide; acetic acid; In acetonitrile; 1.1: Hydrolysis / 2.1: Substitution / 2.2: Acetylation;
DOI:10.1016/s0040-4020(99)00869-8

Reference yield: 60.0%

: nitrate de 3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-4-O-methyl-α,β-D-galactopyranosyle

: 258286-63-4
methyl O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-O-(3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

: C₆₂H₇₄N₁₂O₂₁

: 258286-64-5
C₆₂H₇₄N₁₂O₂₁

Guidance literature:: With de triflate de dimethyl (methylthio) sulfonium; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/s0040-4020(99)00869-8