Technology Process of C21H24N4O4S
There total 4 articles about C21H24N4O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium tert-butylate / toluene / 1.17 h / 20 °C / Cooling with ice
1.2: pH ~ 1
2.1: hydrazine hydrate / methanol / 2.5 h / Reflux
3.1: methanol / 1 h / 20 °C
4.1: hydroxylamine hydrochloride; sodium methylate / methanol / 3 h / 65 °C
5.1: pyridine / acetonitrile; ISOPROPYLAMIDE / 0.72 h / 20 °C
With
pyridine; hydroxylamine hydrochloride; potassium tert-butylate; sodium methylate; hydrazine hydrate;
In
methanol; ISOPROPYLAMIDE; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium methylate / methanol / 3 h / 65 °C
2: pyridine / acetonitrile; ISOPROPYLAMIDE / 0.72 h / 20 °C
With
pyridine; hydroxylamine hydrochloride; sodium methylate;
In
methanol; ISOPROPYLAMIDE; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol / 1 h / 20 °C
2: hydroxylamine hydrochloride; sodium methylate / methanol / 3 h / 65 °C
3: pyridine / acetonitrile; ISOPROPYLAMIDE / 0.72 h / 20 °C
With
pyridine; hydroxylamine hydrochloride; sodium methylate;
In
methanol; ISOPROPYLAMIDE; acetonitrile;