RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)]B(C₆H₅)4

Base Information

• Chemical Name: RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)]B(C₆H₅)4
• CAS No.: 131458-07-6
• Molecular Formula: C₂₄H₂₀B*C₄₂H₄₃N₂P₄Ru
• Molecular Weight: 1120.02

Synonyms:RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)]B(C₆H₅)4

Chemical Property of RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)]B(C₆H₅)4

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Technology Process of RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)]B(C₆H₅)4

There total 4 articles about RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[RuP(CH₂CH₂P(C₆H₅)2)3(H)(N₂)]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(P(CH2CH2P(C6H5)2)3)Ru(H)2 (131458-03-2) + methyl trifluoromethanesulfonate (333-27-7) → [(P(CH2CH2PPh2)3)Ru(H)(η(1)-N2)][BPh4] (131458-07-6)

Guidance literature:

With N₂; In tetrahydrofuran; neat CH3OSO2CF3 was syringed to a soln. of the Ru-compd. under N2, NaBPh4 and EtOH added;;

Reference yield: 80.0%

(P(CH2CH2P(C6H5)2)3)Ru(H)(BH4) + trifluorormethanesulfonic acid (1493-13-6) + sodium tetraphenyl borate (143-66-8) → [(P(CH2CH2PPh2)3)Ru(H)(η(1)-N2)][BPh4] (131458-07-6)

Guidance literature:

In tetrahydrofuran; neat HOSO2CF3 was syringed to a soln. of the Ru-compd. under N2, NaBPh4 was added;;

Reference yield:

{(P(CH2CH2P(C6H5)2)3)Ru(H)(H2)}(1+)*{B(C6H5)4}(1-)={(P(CH2CH2P(C6H5)2)3)Ru(H)(H2)}B(C6H5)4 → [(P(CH2CH2PPh2)3)Ru(H)(η(1)-N2)][BPh4] (131458-07-6)

Guidance literature:

With N₂; In tetrahydrofuran; N2 was bubbled throughout of a soln. of the Ru-compd.; EtOH was added, concd., elem. anal.;;

upstream raw materials:

trifluorormethanesulfonic acid

sodium tetraphenyl borate

(P(CH₂CH₂P(C₆H₅)2)3)Ru(H)2

methyl trifluoromethanesulfonate

Downstream raw materials:

[(P(CH₂CH₂PPh₂)3)Ru(H)(CO)][BPh₄]

{(P(CH₂CH₂P(C₆H₅)2)3)Ru(H)(SO₂)}⁽¹⁺⁾*{B(C₆H₅)4}^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Ru(H)(SO₂)}B(C₆H₅)4

[(P(CH2CH2PPh2)3)Ru(H)(η(2)-C2H4)][BPh4]

{(P(CH₂CH₂P(C₆H₅)2)3)Ru(H)(P(C₂H₅)3)}⁽¹⁺⁾*{B(C₆H₅)4}^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Ru(H)(P(C₂H₅)3)}B(C₆H₅)4

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